CERTIFICATE OF ANALYSIS |
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| | | Report Date | : | 16-Nov-17 |
| | | Expiry Date | : | 8-Nov-19 |
DHM CAS number | 27200-12-0 | Manufacture Date | : | 9-Nov-17 |
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Product Name | Vine Tea Extract | Batch Number | VTE-171109 |
Botanical Source | Ampolopsis grossedentata W.T.Wang. | Batch Quantity | 550kgs |
Plant Part Used | Leaf,100% Natural | Country of Origin | China |
Type of Extraction | Standard Extract | Active Ingredient Markers | Dihydromyricetin |
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Analysis Items | Specifications | Results | Methods used |
Identification | Positive | Conforms | TLC |
Appearance | Fine off-white to white powder | Conforms | Visual test |
Odor & Taste | Characteristic | Conforms | Organoleptic test |
Bulk Density | 45-55g/100ml | Conforms | ASTM D1895B |
Particle Size | 100% through 80 Mesh | Conforms | AOAC 973.03 |
Solubility | Soluble in ethanol & water solution | Conforms | Visual |
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Assay | NLT 98% Dihydromyricetin | 98.09% | HPLC |
Loss on Drying | NMT 5.0% | 1.19% | 5g /105ºC /2hrs |
Ash Content | NMT 5.0% | 0.61% | 2g /525ºC /3hrs |
Extract Solvents | Ethanol & Water | Conforms | / |
Solvent Residues | NMT 0.05% | Conforms | GC |
Excipients | None | Conforms | / |
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Heavy Metals | NMT 10ppm | Conforms | Atomic Absorption |
Arsenic (As) | NMT 2ppm | Conforms | Atomic Absorption |
Lead (Pb) | NMT 2ppm | Conforms | Atomic Absorption |
Cadmium (Cd) | NMT 1ppm | Conforms | Atomic Absorption |
Mercury(Hg) | NMT 0.1ppm | Conforms | Atomic Absorption |
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666 | NMT 0.1ppm | Conforms | USP-GC |
DDT | NMT 0.5ppm | Conforms | USP-GC |
Acephate | NMT 0.2ppm | Conforms | USP-GC |
Methamidophos | NMT 0.2ppm | Conforms | USP-GC |
Parathion-ethyl | NMT 0.2ppm | Conforms | USP-GC |
PCNB | NMT 0.1ppm | Conforms | USP-GC |
Aflatoxins | NMT 0.2ppb | Absent | USP-HPLC |
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Sterilization Method | High temperature & pressure for a short time of 5~10 seconds |
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Microbiological Data | Total Plate Count < 10,000cfu/g | < 1,000cfu/g | GB 4789.2 |
Total Yeast & Mold < 1,000cfu/g | < 50cfu/g | GB 4789.15 |
E. Coli to be negative | Negative | GB 4789.3 |
Staphylococcus to be negative | Negative | GB 4789.10 |
Salmonella to be absent | Absent | GB 4789.4 |
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Packing and Storage | Packed in fiber drum, LDPE bag inside. Net weight: 20kgs/drum. |
Keep away from moisture, strong heat and sunlight. |
Shelf Life | 2 years if sealed and stored in the recommended conditions. |