Item | Standard | Result | ||||
Appearance | White or almost white crystalline powder | Almost white crystalline powder | ||||
Melting point | 152-156°C | 154.6-155.1°C | ||||
Specific optical rotation | -16° to -19° | -17.5° | ||||
Identification | (1)The retention time of the major peak in the chromatogram of the assay preparation corresponds to that in the chromatogram of the standard preparation,as obtained in the assay. | Complies | ||||
(2)UV absorption Max. at 266nm. | Complies | |||||
(3)IR spectra is consistent with CRS. | Complies | |||||
PH | 4.5-6.5 | 5.7 | ||||
Chloride | 0.02% max | <0.02% | ||||
Fluorides | 4.8%min | 4.9% | ||||
Related substances | Individual impurity not more than 0.5% | 0.35% | ||||
Total impurities not more than 2.0% | 0.76% | |||||
Water | 0.5% max | 0.13% | ||||
Residue on ignition | 0.1%max | 0.06% | ||||
Heavy metals | Less than or egual to 20 millionths | Less than20 millionths | ||||
Assay(C12H14Cl2FNO4S) | 98.0%min | 99.0% |
mode of transportation | ||
By Air | By Express | By Sea |
suitable for >50 | suitable for sampple order or <50 | suitable for >300 |
Fast:3-7 days | Fast:3-10 days | Fast: 7-45 days |
lower than the express cost | high shipping cost | lowest cost |